Total synthesis of polyene natural product dihydroxerulin by mild organocatalyzed dehydrogenation of alcohols

  • Hexin Xie
  • , Shilei Zhang
  • , Hao Li
  • , Xinshuai Zhang
  • , Sihan Zhao
  • , Zian Xu
  • , Xixi Song
  • , Xinhong Yu
  • , Wei Wang

Research output: Contribution to journalArticlepeer-review

31 Scopus citations

Abstract

Polyene synthesis: An efficient approach to the total synthesis of polyene natural product dihydroxrulin (1) is described. A novel, mild, direct organocatalytic IBX-mediated dehydrogenation process of simple alcohols to enals has been developed, which serves as a key step in the synthesis (see scheme).

Original languageEnglish (US)
Pages (from-to)2230-2234
Number of pages5
JournalChemistry - A European Journal
Volume18
Issue number8
DOIs
StatePublished - Feb 20 2012
Externally publishedYes

Keywords

  • dehydrogenation
  • dihydroxerulin
  • enals
  • organocatalysis
  • oxidative enamine catalysis
  • polyenes

ASJC Scopus subject areas

  • General Chemistry
  • Catalysis
  • Organic Chemistry

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