Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate

Mehr-Un-Nisa; Munawar Ali Munawar; Gabriel B. Hall; Sue A. Roberts; Victor J. Hruby

doi:10.1107/S1600536812051896

Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate

Mehr-Un-Nisa, Munawar Ali Munawar, Gabriel B. Hall, Sue A. Roberts, Victor J. Hruby

Chemistry and Biochemistry

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

In the title compound, C₁₆H₂2Cl2N₂O ₂, the substituted piperidine ring adopts a chair conformation with both substituents in equatorial positions. In the crystal, N - H⋯O and C - H⋯O hydrogen bonds connect molecules into ribbons along the a-axis direction.

Original language	English (US)
Pages (from-to)	o205
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	69
Issue number	2
DOIs	https://doi.org/10.1107/S1600536812051896
State	Published - Feb 2013

Keywords

R factor = 0.034
T = 100 K
data-to-parameter ratio = 65.3
mean σ(C-C) = 0.001 Å
single-crystal X-ray study
wR factor = 0.079

ASJC Scopus subject areas

Chemistry(all)
Materials Science(all)
Condensed Matter Physics

Access to Document

10.1107/S1600536812051896

Cite this

@article{066cfa6587b34ae38c5ebdd48a253571,

title = "Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate",

abstract = "In the title compound, C16H22Cl2N2O 2, the substituted piperidine ring adopts a chair conformation with both substituents in equatorial positions. In the crystal, N - H⋯O and C - H⋯O hydrogen bonds connect molecules into ribbons along the a-axis direction.",

keywords = "R factor = 0.034, T = 100 K, data-to-parameter ratio = 65.3, mean σ(C-C) = 0.001 {\AA}, single-crystal X-ray study, wR factor = 0.079",

author = "Mehr-Un-Nisa and Munawar, {Munawar Ali} and Hall, {Gabriel B.} and Roberts, {Sue A.} and Hruby, {Victor J.}",

year = "2013",

month = feb,

doi = "10.1107/S1600536812051896",

language = "English (US)",

volume = "69",

pages = "o205",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

number = "2",

}

TY - JOUR

T1 - Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate

AU - Mehr-Un-Nisa,

AU - Munawar, Munawar Ali

AU - Hall, Gabriel B.

AU - Roberts, Sue A.

AU - Hruby, Victor J.

PY - 2013/2

Y1 - 2013/2

N2 - In the title compound, C16H22Cl2N2O 2, the substituted piperidine ring adopts a chair conformation with both substituents in equatorial positions. In the crystal, N - H⋯O and C - H⋯O hydrogen bonds connect molecules into ribbons along the a-axis direction.

AB - In the title compound, C16H22Cl2N2O 2, the substituted piperidine ring adopts a chair conformation with both substituents in equatorial positions. In the crystal, N - H⋯O and C - H⋯O hydrogen bonds connect molecules into ribbons along the a-axis direction.

KW - R factor = 0.034

KW - T = 100 K

KW - data-to-parameter ratio = 65.3

KW - mean σ(C-C) = 0.001 Å

KW - single-crystal X-ray study

KW - wR factor = 0.079

UR - http://www.scopus.com/inward/record.url?scp=84873353153&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84873353153&partnerID=8YFLogxK

U2 - 10.1107/S1600536812051896

DO - 10.1107/S1600536812051896

M3 - Article

C2 - 23424488

AN - SCOPUS:84873353153

VL - 69

SP - o205

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

SN - 1600-5368

IS - 2

ER -

Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate

Abstract

Keywords

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

CCDC 925160: Experimental Crystal Structure Determination

Cite this

Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate

Abstract

Keywords

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Datasets

CCDC 925160: Experimental Crystal Structure Determination

Cite this