Abstract
(Chemical Equation Presented) 1,10-Dimethylbicyclo[8.8.8]hexacosane (1) and 1,10-dihydroxybicyclo[8.8.8]hexacosane (2) were prepared in 4% yield over seven steps and in 18% yield over three steps, respectively, starting from 1,10-cyclooctadecanedione. The identities and out,out conformations of these compounds were established by single-crystal X-ray analysis.
| Original language | English (US) |
|---|---|
| Pages (from-to) | 2841-2843 |
| Number of pages | 3 |
| Journal | Organic Letters |
| Volume | 7 |
| Issue number | 14 |
| DOIs | |
| State | Published - Jul 7 2005 |
ASJC Scopus subject areas
- Biochemistry
- Physical and Theoretical Chemistry
- Organic Chemistry
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Dive into the research topics of 'Synthesis of 1,10-dimethylbicyclo[8.8.8]hexacosane and 1,10- dihydroxybicyclo[8.8.8]hexacosane'. Together they form a unique fingerprint.Datasets
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CCDC 277828: Experimental Crystal Structure Determination
Jones, I. W. (Creator), Monguchi, Y. (Creator), Dawson, A. (Creator), Carducci, M. D. (Creator) & Mash, E. A. (Creator), Cambridge Crystallographic Data Centre, 2005
DOI: 10.5517/cc9b36x, http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/cc9b36x&sid=DataCite
Dataset
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CCDC 277829: Experimental Crystal Structure Determination
Jones, I. W. (Creator), Monguchi, Y. (Creator), Dawson, A. (Creator), Carducci, M. D. (Creator) & Mash, E. A. (Creator), Cambridge Crystallographic Data Centre, 2005
DOI: 10.5517/cc9b37y, http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/cc9b37y&sid=DataCite
Dataset