NiMoO4 selective oxidation catalysts containing excess MoO3 for the conversion of C4 hydrocarbons to maleic anhydride. I. Preparation and characterization

U. Ozkan; G. L. Schrader

doi:10.1016/0021-9517(85)90013-2

NiMoO₄ selective oxidation catalysts containing excess MoO₃ for the conversion of C₄ hydrocarbons to maleic anhydride. I. Preparation and characterization

U. Ozkan, G. L. Schrader

Research output: Contribution to journal › Article › peer-review

93 Scopus citations

Abstract

NiMoO₄ catalysts containing "excess" MoO₃ are active for the selective oxidation of C₄ hydrocarbons to maleic anhydride. The synthesis and characterization of the active component of this catalyst are reported. Synthesis techniques included precipitation, solid-state reaction, and impregnation. Extensive characterization of the catalyst has been performed using complementary instrumentation techniques, including laser Raman spectroscopy, Raman microprobe spectroscopy, X-ray diffraction, X-ray fluorescence, X-ray photoelectron spectroscopy, and scanning electron microscopy.

Original language	English (US)
Pages (from-to)	120-136
Number of pages	17
Journal	Journal of Catalysis
Volume	95
Issue number	1
DOIs	https://doi.org/10.1016/0021-9517(85)90013-2
State	Published - Sep 1985
Externally published	Yes

ASJC Scopus subject areas

Catalysis
Physical and Theoretical Chemistry

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10.1016/0021-9517(85)90013-2

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title = "NiMoO4 selective oxidation catalysts containing excess MoO3 for the conversion of C4 hydrocarbons to maleic anhydride. I. Preparation and characterization",

abstract = "NiMoO4 catalysts containing {"}excess{"} MoO3 are active for the selective oxidation of C4 hydrocarbons to maleic anhydride. The synthesis and characterization of the active component of this catalyst are reported. Synthesis techniques included precipitation, solid-state reaction, and impregnation. Extensive characterization of the catalyst has been performed using complementary instrumentation techniques, including laser Raman spectroscopy, Raman microprobe spectroscopy, X-ray diffraction, X-ray fluorescence, X-ray photoelectron spectroscopy, and scanning electron microscopy.",

author = "U. Ozkan and Schrader, {G. L.}",

note = "Funding Information: This work was conductedt hrought he Ames Laboratory which is operated for the U.S. Departmento f Energy by Iowa State University under Contract W-740%ENG-82.T he X-ray photoelectrons pectroscopy work by James W. Anderegg and Guinier camera X-ray diffractione xperimentsb y Bernd U. Harbrechta re gratefully acknowledged.",

year = "1985",

month = sep,

doi = "10.1016/0021-9517(85)90013-2",

language = "English (US)",

volume = "95",

pages = "120--136",

journal = "Journal of Catalysis",

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T1 - NiMoO4 selective oxidation catalysts containing excess MoO3 for the conversion of C4 hydrocarbons to maleic anhydride. I. Preparation and characterization

AU - Ozkan, U.

AU - Schrader, G. L.

N1 - Funding Information: This work was conductedt hrought he Ames Laboratory which is operated for the U.S. Departmento f Energy by Iowa State University under Contract W-740%ENG-82.T he X-ray photoelectrons pectroscopy work by James W. Anderegg and Guinier camera X-ray diffractione xperimentsb y Bernd U. Harbrechta re gratefully acknowledged.

PY - 1985/9

Y1 - 1985/9

N2 - NiMoO4 catalysts containing "excess" MoO3 are active for the selective oxidation of C4 hydrocarbons to maleic anhydride. The synthesis and characterization of the active component of this catalyst are reported. Synthesis techniques included precipitation, solid-state reaction, and impregnation. Extensive characterization of the catalyst has been performed using complementary instrumentation techniques, including laser Raman spectroscopy, Raman microprobe spectroscopy, X-ray diffraction, X-ray fluorescence, X-ray photoelectron spectroscopy, and scanning electron microscopy.

AB - NiMoO4 catalysts containing "excess" MoO3 are active for the selective oxidation of C4 hydrocarbons to maleic anhydride. The synthesis and characterization of the active component of this catalyst are reported. Synthesis techniques included precipitation, solid-state reaction, and impregnation. Extensive characterization of the catalyst has been performed using complementary instrumentation techniques, including laser Raman spectroscopy, Raman microprobe spectroscopy, X-ray diffraction, X-ray fluorescence, X-ray photoelectron spectroscopy, and scanning electron microscopy.

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NiMoO₄ selective oxidation catalysts containing excess MoO₃ for the conversion of C₄ hydrocarbons to maleic anhydride. I. Preparation and characterization

Abstract

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